- Synthesis of Zr-Ti Alloy Powder by Magnesium Reduction
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Dong-Won Lee, Geun-Tae Park, Tae-Soo Lim, Hye-Moon Lee, Ji-Hun Yu
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J Korean Powder Metall Inst. 2011;18(4):359-364.
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DOI: https://doi.org/10.4150/KPMI.2011.18.4.359
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- Zr-Ti alloy powders were successfully synthesized by magnesium thermal reduction of metal chlorides. The evaporated and mixed gasses of ZrCl_4+TiCl_4 were injected to liquid magnesium and the chloride components were reduced by magnesium leading to the formation of MgCl_2. The released Zr and Ti atoms were then condensed to particle forms inside the mixture of liquid magnesium and magnesium chloride, which could be dissolved fully in post process by 1~5% HCl solution at room temperature. By the fraction-control of individually injected ZrCl_4 and TiCl_4 gasses, the final compositions of produced alloy powders were changed in the ranges of Zr-0 wt.%~20 wt.%Ti and their purity and particle size were about 99.4% and the level of several micrometers, respectively.
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Citations
Citations to this article as recorded by  - Synthesis of Vanadium Powder by Magnesiothermic Reduction
Dong Won Lee, Hak Sung Lee, Jung Yeul Yun, Young Ho Kim, Jei Pil Wang
Advanced Materials Research.2014; 1025-1026: 509. CrossRef - Extraction of Vanadium Powder by Metallothermic Reduction
Dong-Won Lee, Sang-Hyun Heo, Jong-Taek Yeom, Jei-Pil Wang
Journal of Korean Powder Metallurgy Institute.2013; 20(1): 43. CrossRef
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